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Preparation of Strontium Bismuth Tantalum (SBT) Fine Powder by Sol-Gel Process Using Bismuth Subnitrate as Bismuth Source

Wen WANG , Yu ZHOU , Sheng CHEN , Feng Y , Dechang JIA

材料科学技术(英)

Strontium bismuth tantalum (SBT) fine power was prepared by Sol-Gel method. Pentaethoxy tantalum, strontium acetate and bismuth subnitrate were used as raw materials, and were dissolved in proper order in ethylene glycol to form transparent sol. The mixed precursor was dried at 80℃ and annealed at 800℃ for 1 h. Crystallized nanometer sized SBT fine powder was obtained and characterized by XRD.

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Variations of Microstructure and Mechanical Properties of Si-B-O-N Ceramics with Sintering Temperatures

Junbao ZHANG , Guangwu WEN , Tingquan LEI , Dechang JIA , Jiancun RAO

材料科学技术(英)

Si-B-O-N powder without B-O bonds synthesized by polymeric precursor were hot-pressed into ceramics at different temperatures. The variations of microstructure and mechanical properties of Si-B-O-N ceramics have been investigated. Crystallization of Si-B-O-N ceramics occurred at about 1400°C. Density, elastic modulus, and flexural strength of the ceramics increased with the increasing sintering temperatures, and reached to their maximum values at 1600°C. By contrast,hardness and fracture toughness of the ceramics monotonically changed with increasing sintering temperatures. Hardness decreased, while the fracture toughness increased. The principal toughening mechanisms including crack deflection, crack bridging and plate grain pulling-out effects are discussed

关键词: Si-B-O-N ceramics , null , null , null

Corrosion Resistance of Plasma Sprayed Ceramic Composite Coatings on Q235 Substrate

Dianran YAN , Jining HE , XiangZhi LI , Yangai LIU , Yu ZHOU , Dechang JIA

材料科学技术(英)

The corrosion resistance of SiO2/A12O3, TiO2/Al2O3 and (SiO2+TiO2)/Al2O3 ceramic composite coatings on Q235 substrate fabricated by means of plasma spraying was investigated. The results show that A12O3+13 wt pct TiO2 ceramic coating has the highest density, the lowest connected porosity and the best corrosion resistance. The corrosion mechanism of Q235 with ceramic coating has also been studied.

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